Simultaneous determination of local thickness and composition for ternary III-V semiconductors by aberration-corrected STEM

Scanning transmission electron microscopy (STEM) is a suitable method for the quantitative characterization of nanomaterials. For an absolute composition determination on an atomic scale, the thickness of the specimen has to be known locally with high accuracy. Here, we propose a method to determine...

全面介绍

Gespeichert in:
书目详细资料
Autoren: Kükelhan, Pirmin, Beyer, Andreas, Firoozabadi, Saleh, Hepp, Thilo, Volz, Kerstin
格式: 文件
语言:英语
出版: Philipps-Universität Marburg 2019
主题:
在线阅读:PDF-Volltext
标签: 添加标签
没有标签, 成为第一个标记此记录!
实物特征
总结:Scanning transmission electron microscopy (STEM) is a suitable method for the quantitative characterization of nanomaterials. For an absolute composition determination on an atomic scale, the thickness of the specimen has to be known locally with high accuracy. Here, we propose a method to determine both thickness and composition of ternary III-V semiconductors locally from one STEM image as shown for the example material systems Ga(AsBi) and (GaIn)As. In a simulation study, the feasibility of the method is proven and the influence of specimen thickness and detector angles used is investigated. An application to an experimental STEM image of a Ga(AsBi) quantum well grown by metal organic vapour phase epitaxy yields an excellent agreement with composition results from high resolution X-ray diffraction.
实物描述:31 Seiten
DOI:10.17192/es2021.0022